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ChemicalBook CAS DataBase List (3-BROMO-PYRIDIN-2-YL)-METHYL-AMINE

(3-BROMO-PYRIDIN-2-YL)-METHYL-AMINE synthesis

1synthesis methods
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Yield:214977-38-5 87%

Reaction Conditions:

Stage #1: 2-Amino-3-bromopyridinewith sodium hydride in tetrahydrofuran at 40; for 0.5 h;
Stage #2: iodomethane in tetrahydrofuran at 40 - 60;Further stages.;

References:

Patriciu, Oana-Irina;Pillard, Christelle;Finaru, Adriana-Luminita;Sandulescu, Ioan;Guillaumet, Gerald [Synthesis,2007,# 24,p. 3868 - 3876]

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