![](/CAS/20180906/GIF/1357946-60-1.gif)
3-c]pyridine synthesis
- Product Name:3-c]pyridine
- CAS Number:1357946-60-1
- Molecular formula:C7H7N3
- Molecular Weight:133.15
![1H-Pyrazolo[4,3-c]pyridine,4-chloro-6-Methyl-](/CAS/GIF/1159828-70-2.gif)
1159828-70-2
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$45.00/5mg
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Yield:-
Reaction Conditions:
with hydrogen;palladium 10% on activated carbon in tetrahydrofuran;ethanol at 20; for 24 h;
Steps:
A solution of 4-chloro-6-methyl-1 H-pyrazolo[4,3-c]pyridine [1159828-70-2] (750 mg, 4.48 mmol) in a mixture of ethanol (25 mL) and THF (10 mL) was hydrogenated over 10% Pd/C (75 mg, 0.07 mmol) at RT for 24 h. The reaction mixture was filtered, the catalyst was washed with ethanol and the filtrate was concentrated under vacuum. MS (LC-MS): 134 [M+H]+, tR (HPLC conditions k): 0.23 min.
References:
WO2012/93101,2012,A1 Location in patent:Page/Page column 159
![4-CHLORO-6-METHYL-NICOTINIC ACID METHYL ESTER](/CAS/GIF/886372-05-0.gif)
886372-05-0
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$75.00/100mg
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1357946-60-1
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![CHEMBRDG-BB 4002882](/CAS/GIF/33821-58-8.gif)
33821-58-8
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$46.00/1g
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![4-chloro-6-methylnicotinoyl chloride](/CAS/20180703/GIF/1005515-30-9.gif)
1005515-30-9
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![3-c]pyridine](/CAS/20180906/GIF/1357946-60-1.gif)
1357946-60-1
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