3-CHLOROPHENYL CYCLOPROPYL KETONE synthesis
- Product Name:3-CHLOROPHENYL CYCLOPROPYL KETONE
- CAS Number:898789-97-4
- Molecular formula:C10H9ClO
- Molecular Weight:180.63
108-37-2
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$6.00/10g
5500-21-0
303 suppliers
$16.00/5mL
898789-97-4
16 suppliers
$417.00/1g
Yield: 68%
Reaction Conditions:
Stage #1:1-bromo-3-chlorobenzene with n-butyllithium in hexane at 0 - 20; for 4 h;Inert atmosphere;
Stage #2:cyclopropropanecarbonitrile in hexane at 20; for 0.166667 h;Inert atmosphere;
Stage #3: with toluene-4-sulfonic acid in hexane;water at 20; for 0.5 h;Inert atmosphere;
References:
Huang, Huawen;Ji, Xiaochen;Wu, Wanqing;Jiang, Huanfeng [Chemical Communications,2013,vol. 49,# 32,p. 3351 - 3353] Location in patent:supporting information
108-37-2
356 suppliers
$6.00/10g
147356-78-3
86 suppliers
$25.00/1g
898789-97-4
16 suppliers
$417.00/1g