3-Chlorophenylisopropyl ketone synthesis
- Product Name:3-Chlorophenylisopropyl ketone
- CAS Number:55649-98-4
- Molecular formula:C10H11ClO
- Molecular Weight:182.65
120127-00-6
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55649-98-4
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Yield:55649-98-4 450 mg
Reaction Conditions:
Stage #1: C10H13ClOwith oxalyl dichloride in dichloromethane;dimethyl sulfoxide at -78; for 1 h;Inert atmosphere;
Stage #2: with triethylamine in dichloromethane;dimethyl sulfoxide at 20;
References:
Lackner, Aaron D.;Samant, Andrew V.;Toste, F. Dean [Journal of the American Chemical Society,2013,vol. 135,# 38,p. 14090 - 14093] Location in patent:supporting information
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55649-98-4
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55649-98-4
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