3-FLUORO-2-TRIMETHYLSILANYL-PYRIDINE synthesis
- Product Name:3-FLUORO-2-TRIMETHYLSILANYL-PYRIDINE
- CAS Number:87674-09-7
- Molecular formula:C8H12FNSi
- Molecular Weight:169.27
372-47-4
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$5.00/1g
75-77-4
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77332-77-5
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87674-09-7
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$295.00/1g
Yield:87674-09-7 68% ，77332-77-5 3%
Reaction Conditions:
with n-butyllithium;N,N,N,N,-tetramethylethylenediamine in diethyl ether at -40; for 0.5 h;Product distribution;other solvent, temperatures and reaction times, instead of TMEDA with DABCO, LDA and various excess of LDA;
References:
Marsais, Francis;Queguiner, Guy [Tetrahedron,1983,vol. 39,# 12,p. 2009 - 2021]