3-FLUOROBENZYLZINC CHLORIDE synthesis
- Product Name:3-FLUOROBENZYLZINC CHLORIDE
- CAS Number:312693-06-4
- Molecular formula:C7H6ClFZn
- Molecular Weight:209.96
456-42-8
329 suppliers
$5.00/5g
7646-85-7
536 suppliers
$10.00/25ml
312693-06-4
24 suppliers
$232.00/50ml
Yield:312693-06-4 66%
Reaction Conditions:
Stage #1: zinc(II) chloridewith lithium chloride at 320 - 450; for 0.166667 h;Inert atmosphere;Schlenk technique;
Stage #2: m-fluorobenzyl chloridewith magnesium in tetrahydrofuran at 20; for 2 h;Inert atmosphere;Schlenk technique;
References:
Benischke, Andreas D.;Knoll, Irina;Rérat, Alice;Gosmini, Corinne;Knochel, Paul [Chemical Communications,2016,vol. 52,# 15,p. 3171 - 3174] Location in patent:supporting information