2-CHLOROBENZYLZINC CHLORIDE synthesis
- Product Name:2-CHLOROBENZYLZINC CHLORIDE
- CAS Number:312624-11-6
- Molecular formula:C7H6Cl2Zn
- Molecular Weight:226.42
611-19-8
429 suppliers
$7.00/25g
7646-85-7
536 suppliers
$10.00/25ml
312624-11-6
15 suppliers
$286.00/50ml
Yield:312624-11-6 81%
Reaction Conditions:
Stage #1: zinc(II) chloridewith lithium chloride at 320 - 450; for 0.166667 h;Inert atmosphere;Schlenk technique;
Stage #2: 1-chloro-2-(chloromethyl)benzenewith magnesium in tetrahydrofuran at 20; for 1 h;Inert atmosphere;Schlenk technique;
References:
Benischke, Andreas D.;Knoll, Irina;Rérat, Alice;Gosmini, Corinne;Knochel, Paul [Chemical Communications,2016,vol. 52,# 15,p. 3171 - 3174] Location in patent:supporting information
611-19-8
429 suppliers
$7.00/25g
7440-66-6
11 suppliers
$14.00/5g
312624-11-6
15 suppliers
$286.00/50ml