3-Hydroxy-2-methylpropyl 4-methylbenzenesulfonate synthesis
- Product Name:3-Hydroxy-2-methylpropyl 4-methylbenzenesulfonate
- CAS Number:1019030-46-6
- Molecular formula:C11H16O4S
- Molecular Weight:244.31
Yield:1019030-46-6 70%
Reaction Conditions:
Stage #1: 2-methyl-1.3-propanediolwith pyridine in dichloromethane at 0;Inert atmosphere;
Stage #2: p-toluenesulfonyl chloride in dichloromethane at 0; for 3 h;Inert atmosphere;
References:
Bolla, R. Sekhar;Kasi Viswanath [Journal of labelled compounds and radiopharmaceuticals,2014,vol. 57,# 2,p. 82 - 85]
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