3-Hydroxy-2-methylpyridine synthesis
- Product Name:3-Hydroxy-2-methylpyridine
- CAS Number:1121-25-1
- Molecular formula:C6H7NO
- Molecular Weight:109.13
1192-62-7
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1121-25-1
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: NH2OH*HCl, NaOH / ethanol; H2O / 0.33 h / Heating
2: Raney Ni alloy, 2 N aq. NaOH / ethanol / 1 h / Ambient temperature
3: 1.) oxygen, tetraphenylporphine, 2.) triphenylphosphine / 1.) CH2Cl2, -70 deg C, irradiation, 2 h, 2.) -70 deg C, 10 min
References:
Kuo;Shih [Chemical and Pharmaceutical Bulletin,1991,vol. 39,# 1,p. 181 - 183]
109-06-8
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1121-25-1
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$8.00/250mg
1000414-75-4
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1121-25-1
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1072088-64-2
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2168-13-0
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$12.00/1mg
1121-25-1
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$8.00/250mg