3-Methoxy-6-Nitro-2-Picoline synthesis
- Product Name:3-Methoxy-6-Nitro-2-Picoline
- CAS Number:23904-02-1
- Molecular formula:C7H8N2O3
- Molecular Weight:168.15
1628-89-3
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Yield:-
Reaction Conditions:
with nitric acid in sulfuric acid;
Steps:
A.9.b Example A9
b) The methoxypyridine (24.2 g) was dissolved in concentrated sulphuric acid (100 ml) and treated with a mixture of concentrated nitric acid (16.5 ml) and concentrated sulphuric acid (20.0 ml) which was added dropwise with stirring at 5° C., to give 3-methoxy-2-methyl-6-nitropyridine, m.p. 96°-98° C.
References:
US5464781,1995,A
26395-26-6
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23904-02-1
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