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ChemicalBook CAS DataBase List 3-METHYL-4-OCTANONE

3-METHYL-4-OCTANONE synthesis

10synthesis methods
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Yield:20754-04-5 92%

Reaction Conditions:

Stage #1: n-butyl magnesium bromidewith cerium(III) chloride in tetrahydrofuran at -78; for 2 h;
Stage #2: 2-methyl-1-morpholin-4-ylbutan-1-one in tetrahydrofuran at -78; for 1.5 h;Further stages.;

References:

Badioli, Michele;Ballini, Roberto;Bartolacci, Massimo;Bosica, Giovanna;Torregiani, Elisabetta;Marcantoni, Enrico [Journal of Organic Chemistry,2002,vol. 67,# 25,p. 8938 - 8942]

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