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3-Phenylisonicotinonitrile synthesis

5synthesis methods
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Yield:36146-27-7 87 %

Reaction Conditions:

Stage #1: 3-bromo-4-cyanopyridine;phenylboronic acidwith potassium carbonate;triphenylphosphine in water;Inert atmosphere;Suzuki-Miyaura Coupling;
Stage #2: with palladium diacetate in 1,2-dimethoxyethane;water;Inert atmosphere;Glovebox;Reflux;

References:

Vaid, Thomas P.;Cook, Monique E.;Scott, Jessica D.;Borjesson Carazo, Marino;Ruchti, Jonathan;Minteer, Shelley D.;Sigman, Matthew S.;McNeil, Anne J.;Sanford, Melanie S. [Chemistry - A European Journal,2022,vol. 28,# 70,art. no. E202202147]

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39065-43-5 Synthesis
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36146-27-7
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