ChemicalBook CAS DataBase List 5-Chloro-6'-Methyl-3-[4-(Methylsulfonyl)phenyl]-2,3'-bipyridine 1'-Oxide

5-Chloro-6'-Methyl-3-[4-(Methylsulfonyl)phenyl]-2,3'-bipyridine 1'-Oxide synthesis

2synthesis methods

Product Name:5-Chloro-6'-Methyl-3-[4-(Methylsulfonyl)phenyl]-2,3'-bipyridine 1'-Oxide
CAS Number:325855-74-1
Molecular formula:C18H15ClN2O3S
Molecular Weight:374.84

221615-75-4 Synthesis

1-(6-Methylpyridin-3-yl)-2-(4-(methylsulfonyl)phenyl)ethanone

221615-75-4
267 suppliers
$8.00/250mg

5-Chloro-6'-Methyl-3-[4-(Methylsulfonyl)phenyl]-2,3'-bipyridine 1'-Oxide

325855-74-1
64 suppliers
$125.00/50mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: t-BuOK / tetrahydrofuran / 0.75 h / 20 °C
1.2: 85 percent / AcOH; TFA; NH₂OH*HCl / tetrahydrofuran; H₂O / 5 h / Heating
2.1: 89 percent / mCPBA

References:

Davies, Ian W.;Marcoux, Jean-Francois;Reider, Paul J. [Organic Letters,2001,vol. 3,# 2,p. 209 - 211]

202409-33-4
532 suppliers
$5.00/10mg

325855-74-1
64 suppliers
$125.00/50mg

References

5-Chloro-6'-Methyl-3-[4-(Methylsulfonyl)phenyl]-2,3'-bipyridine 1'-Oxide Related Search:

1-(6-Methylpyridin-3-yl)-2-(4-(Methylthio)phenyl)ethanone 3,5-Dichloropyridine 4-Methylsulphonylphenylacetic acid 1-(6-Methylpyridin-3-yl)-2-(4-(methylsulfonyl)phenyl)ethanone Methyl 6-methylnicotinate 6-Methylnicotinic acid 4-methylsulfinylbenzoate