ChemicalBook CAS DataBase List S-6-(tert-butoxycarbonyl)-5,6-dihydro-6H-[1,4]diazepino[6,7,1-hi]indole

S-6-(tert-butoxycarbonyl)-5,6-dihydro-6H-[1,4]diazepino[6,7,1-hi]indole synthesis

6synthesis methods

Product Name:S-6-(tert-butoxycarbonyl)-5,6-dihydro-6H-[1,4]diazepino[6,7,1-hi]indole
CAS Number:345264-15-5
Molecular formula:C16H20N2O2
Molecular Weight:272.34

1074-88-0
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S-6-(tert-butoxycarbonyl)-5,6-dihydro-6H-[1,4]diazepino[6,7,1-hi]indole

345264-15-5
14 suppliers
$775.00/1g

Yield:-

Steps:

Multi-step reaction with 4 steps
1: H₂ / Pd/c / methanol / 20 °C / 760 Torr
2: aq. K₂CO₃ / tetrahydrofuran / 0 °C
3: Et₃N / tetrahydrofuran / 2 h / 0 °C
4: NaH / dimethylformamide / 0 °C

References:

Engler, Thomas A.;Henry, James R.;Malhotra, Sushant;Cunningham, Brian;Furness, Kelly;Brozinick, Joseph;Burkholder, Timothy P.;Clay, Michael P.;Clayton, Joshua;Diefenbacher, Clive;Hawkins, Eric;Iversen, Philip W.;Li, Yihong;Lindstrom, Terry D.;Marquart, Angela L.;McLean, Johnathan;Mendel, David;Misener, Elizabeth;Briere, Daniel;O'Toole, John C.;Porter, Warren J.;Queener, Steven;Reel, Jon K.;Owens, Rebecca A.;Brier, Richard A.;Eessalu, Thomas E.;Wagner, Jill R.;Campbell, Robert M.;Vaughn, Renee [Journal of Medicinal Chemistry,2004,vol. 47,# 16,p. 3934 - 3937]

Ethanol, 2-[(1H-indol-7-ylmethyl)amino]-

408356-56-9
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345264-15-5
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References

Carbamic acid, N-(2-hydroxyethyl)-N-(1H-indol-7-ylmethyl)-, 1,1-dimethylethyl ester

748811-02-1
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345264-15-5
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References

13708-58-2
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$90.00/50mg

345264-15-5
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References

46006-95-5 Synthesis

46006-95-5
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345264-15-5
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References