ChemicalBook CAS DataBase List 4-(3,4-difluorophenyl)cyclohexanone

4-(3,4-difluorophenyl)cyclohexanone synthesis

2synthesis methods

Product Name:4-(3,4-difluorophenyl)cyclohexanone
CAS Number:135862-41-8
Molecular formula:C12H12F2O
Molecular Weight:210.22

1,4-DIOXA-SPIRO[4,5]DEC-7-EN-8-BORONIC ACID, PINACOL ESTER

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C
2: trifluoroacetic acid / dichloromethane / 20 °C
3: palladium 10% on activated carbon; hydrogen / ethyl acetate / 6 h / 20 °C / 3000.3 Torr

References:

WO2018/54365,2018,A1

64248-58-4
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$14.00/5g

135862-41-8
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References

4-(3,4-difluorophenyl)cyclohexanone Related Search:

4-(1',1''-BIPHENYL-4'-YL)-CYCLOHEXANONE