4,4-di-n-hexyl-dithieno[3,2-b:2',3'-d]silole synthesis
- Product Name:4,4-di-n-hexyl-dithieno[3,2-b:2',3'-d]silole
- CAS Number:906372-08-5
- Molecular formula:C20H30S2Si
- Molecular Weight:362.67
51751-44-1
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18204-93-8
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Yield:906372-08-5 68%
Reaction Conditions:
Stage #1: 3,3'dibromo-2,2'-bithiophenewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1.5 h;
Stage #2: dichlorodi-n-hexylsilane in tetrahydrofuran;hexane at -78 - 20;
References:
Usta, Hakan;Lu, Gang;Facchetti, Antonio;Marks, Tobin J. [Journal of the American Chemical Society,2006,vol. 128,# 28,p. 9034 - 9035]
125143-53-5
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906372-08-5
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492-97-7
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$5.00/1g
906372-08-5
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