4,4'-DIBROMODIPHENYL-D8 synthesis
- Product Name:4,4'-DIBROMODIPHENYL-D8
- CAS Number:80523-79-1
- Molecular formula:C12Br2D8
- Molecular Weight:320.05
4165-56-4
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$36.00/1g
80523-79-1
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$160.00/25mg
Yield:80523-79-1 75%
Reaction Conditions:
Stage #1: 1,4-dibromotetradeuterobenzenewith tert.-butyl lithium in tetrahydrofuran at -78; for 1.5 h;
Stage #2: with copper(l) cyanide in tetrahydrofuran at -78 - 20;
Stage #3: with 2,5-Dimethyl-1,4-benzoquinone in tetrahydrofuran at 20; for 3 h;
References:
Obrien, Zachary J.;Karlen, Steven D.;Khan, Saeed;Garcia-Garibay, Miguel A. [Journal of Organic Chemistry,2010,vol. 75,# 8,p. 2482 - 2491] Location in patent:experimental part
142475-00-1
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inquiry
80523-79-1
15 suppliers
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1486-01-7
44 suppliers
$108.00/1g
80523-79-1
15 suppliers
$160.00/25mg
1486-01-7
44 suppliers
$108.00/1g
142475-00-1
9 suppliers
inquiry
80523-79-1
15 suppliers
$160.00/25mg