![](/CAS/GIF/101-63-3.gif)
4,4'-DINITRODIPHENYL ETHER synthesis
- Product Name:4,4'-DINITRODIPHENYL ETHER
- CAS Number:101-63-3
- Molecular formula:C12H8N2O5
- Molecular Weight:260.2
![Potassium benzoate](/CAS/GIF/582-25-2.gif)
582-25-2
335 suppliers
$5.00/25g
![4-Fluoronitrobenzene](/CAS/GIF/350-46-9.gif)
350-46-9
513 suppliers
$10.60/1gm:
![4,4'-DINITRODIPHENYL ETHER](/CAS/GIF/101-63-3.gif)
101-63-3
106 suppliers
$10.00/1g
Yield:101-63-3 98.5%
Reaction Conditions:
with sodium carbonate in ISOPROPYLAMIDE
Steps:
7 EXAMPLE 7
EXAMPLE 7 A 250 ml flask equipped with an agitator, thermometer, and nitrogen bleed is charged with 66.5 (0.47 mole) p-fluoronitrobenzene, 77 g dimethylacetamide, 0.57 g (0.004 mole) potassium benzoate and 25 g (0.24 mole) sodium carbonate. The reaction mixture is heated to and maintained at 170° C. while it is agitated and kept under a nitrogen blanket. After 12 hours 4,4'-dinitrodiphenyl ether is obtained in 98.5% yield.
References:
E. I. Du Pont de Nemours and Company US4558164, 1985, A
![4-Chloronitrobenzene](/CAS/GIF/100-00-5.gif)
100-00-5
8 suppliers
$14.00/25g
![4,4'-DINITRODIPHENYL ETHER](/CAS/GIF/101-63-3.gif)
101-63-3
106 suppliers
$10.00/1g
![Mesityl(4-nitrophenyl)iodonium triflate](/CAS/20180808/GIF/1146127-11-8.gif)
1146127-11-8
7 suppliers
$114.00/1g
![4-Nitrophenylboronic acid](/CAS/GIF/24067-17-2.gif)
24067-17-2
249 suppliers
$19.00/1g
![4,4'-DINITRODIPHENYL ETHER](/CAS/GIF/101-63-3.gif)
101-63-3
106 suppliers
$10.00/1g
![(4-Nitrophenyl)phenyliodonium trifluoromethanesulfonate](/CAS/20180808/GIF/905718-45-8.gif)
905718-45-8
23 suppliers
$23.30/25MG
![4,4'-DINITRODIPHENYL ETHER](/CAS/GIF/101-63-3.gif)
101-63-3
106 suppliers
$10.00/1g