ChemicalBook CAS DataBase List 4,5,6,7-TETRAHYDRO-BENZO[D]ISOXAZOL-3-OL

4,5,6,7-TETRAHYDRO-BENZO[D]ISOXAZOL-3-OL synthesis

3synthesis methods

Product Name:4,5,6,7-TETRAHYDRO-BENZO[D]ISOXAZOL-3-OL
CAS Number:27772-90-3
Molecular formula:C7H9NO2
Molecular Weight:139.15

1655-07-8 Synthesis

1655-07-8
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4,5,6,7-TETRAHYDRO-BENZO[D]ISOXAZOL-3-OL

27772-90-3
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Yield:-

Reaction Conditions:

Stage #1: ethyl 2-oxocyclohexane carboxylatewith sodium hydroxide;hydroxylamine hydrochloride in methanol;water at -70 - 0; for 2 h;
Stage #2: with hydrogenchloride in methanol;water;acetone;Reflux;

References:

Clausen, Rasmus P.;Naur, Peter;Kristensen, Anders S.;Greenwood, Jeremy R.;Strange, Mette;Brauner-Osborne, Hans;Jensen, Anders A.;Nielsen, Anne Sophie T.;Geneser, Ulla;Ringgaard, Lone M.;Nielsen, Birgitte;Pickering, Darryl S.;Brehm, Lotte;Gajhede, Michael;Krogsgaard-Larsen, Povl;Kastrup, Jette S. [Journal of Medicinal Chemistry,2009,vol. 52,# 15,p. 4911 - 4922] Location in patent:scheme or table

1,4-Dioxaspiro[4.5]decane-6-carboxamide,N-hydroxy-

27773-01-9
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27772-90-3
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References

1655-07-8 Synthesis

1655-07-8
304 suppliers
$6.00/5g

27772-90-3
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2,1-Benzisoxazol-3(3aH)-one, 4,5,6,7-tetrahydro-

29879-44-5
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References

4,5,6,7-TETRAHYDRO-BENZO[D]ISOXAZOL-3-OL Related Search:

BENZO[D]ISOXAZOL-3-OL