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ChemicalBook CAS DataBase List 4,5-DIMETHOXY-1-INDANONE

4,5-DIMETHOXY-1-INDANONE synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: piperidinium acetate / ethanol / 0.5 h
1.2: 44 percent / NaBH3CN / ethanol / 0 - 20 °C
2.1: 64 percent / Sc(OTf)3 / nitromethane / 1.33 h / 100 °C

References:

Fillion, Eric;Fishlock, Dan;Wilsily, Ashraf;Goll, Julie M. [Journal of Organic Chemistry,2005,vol. 70,# 4,p. 1316 - 1327]

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