4-acetylphenylacetonitrile synthesis

13synthesis methods

Product Name:4-acetylphenylacetonitrile
CAS Number:10266-42-9
Molecular formula:C10H9NO
Molecular Weight:159.18

928664-98-6 Synthesis

928664-98-6
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99-90-1
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10266-42-9
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Yield:10266-42-9 86%

Reaction Conditions:

with (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;potassium fluoride;water in dimethyl sulfoxide at 130; for 16 h;Inert atmosphere;Domino Suzuki coupling and fragmentation reaction;

References:

Velcicky, Juraj;Soicke, Arne;Steiner, Roland;Schmalz, Hans-Guenther [Journal of the American Chemical Society,2011,vol. 133,# 18,p. 6948 - 6951] Location in patent:supporting information; experimental part

16532-79-9 Synthesis