4-AMINO-2,2-DIMETHYL-BUTYRIC ACID synthesis

1synthesis methods

Product Name:4-AMINO-2,2-DIMETHYL-BUTYRIC ACID
CAS Number:138146-22-2
Molecular formula:C6H13NO2
Molecular Weight:131.17

Spiro[2,4-benzodioxepin-3,1'-cyclopropane]-2'-carbonitrile, 1,5-dihydro-3',3'-dimethyl-

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138146-22-2
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Yield:138146-22-2 91%

Reaction Conditions:

Stage #1:C₁₄H₁₅NO₂ with hydrogen;palladium on activated charcoal in ethyl acetate under 750.075 Torr; for 24 h;
Stage #2: with hydrogen;acetic acid;palladium on activated charcoal;trimethyleneglycol under 2250.23 Torr; for 72 h;Further stages.;

References:

Royer;Felpin;Doris [Journal of Organic Chemistry,2001,vol. 66,# 19,p. 6487 - 6489]

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