4-AMINOBUTYRIC-2,2-D2 ACID synthesis
- Product Name:4-AMINOBUTYRIC-2,2-D2 ACID
- CAS Number:67910-98-9
- Molecular formula:C4H7D2NO2
- Molecular Weight:105.13
1204763-35-8
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67910-98-9
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Yield:67910-98-9 48%
Reaction Conditions:
Stage #1: ethyl [2,2,3,3-(2)H4]-3-cyanopropanoatewith water;sodium hydroxide for 1.5 h;Reflux;
Stage #2: with sodium borodeuteride;cobalt(II) chloride hexahydrate
References:
Cook, Matthew C.;Witherell, Ross D.;White, Robert L. [Letters in drug design and discovery,2010,vol. 7,# 1,p. 9 - 13] Location in patent:experimental part