4-Benzothiazolamine,2-methyl-(9CI) synthesis

5synthesis methods

Product Name:4-Benzothiazolamine,2-methyl-(9CI)
CAS Number:10023-33-3
Molecular formula:C8H8N2S
Molecular Weight:164.23

Benzothiazole, 2-methyl-4-nitro- (6CI,7CI)

90196-40-0
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10023-33-3
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Yield:10023-33-3 0.94 g

Reaction Conditions:

with palladium on activated charcoal;hydrogen in methanol;

Steps:

G

[00314] 1.27 g of 2-methyl-4-nitro-1 ,3-benzothiazole was hydrogenated over 0.13 g Pd/C catalyst in 150 mL methanol. Filtration and evaporation gave 0.94 g 2-methyl-1 ,3-benzothiazol- 4-amine.

References:

WO2014/113492,2014,A2 Location in patent:Paragraph 00314

13382-43-9 Synthesis

13382-43-9
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10023-33-3
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References

Acetamide, N-(2-methyl-5-benzothiazolyl)- (9CI)

68867-15-2
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10023-33-3
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Acetamide, N-(2-methyl-4-nitro-5-benzothiazolyl)-

103261-81-0
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10023-33-3
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5-Benzothiazolamine,2-methyl-4-nitro-(9CI)

40671-24-7
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10023-33-3
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References