4-bromo-2-methylpyridine 1-oxide synthesis
- Product Name:4-bromo-2-methylpyridine 1-oxide
- CAS Number:100367-74-6
- Molecular formula:C6H6BrNO
- Molecular Weight:188.02
Yield: 31%
Steps:
67.a a
a 4-Bromo-2-picoline N-oxide 4-Nitro-2-picoline N-oxide (1.0 g, 6.5 mmol) was treated with acetyl bromide (3.5 mL, 47 mmol) as described in Example 65b to provide the title compound (0.38 g, 31%) as an orange-brown oil.
References:
Boehringer Ingelheim Pharmaceuticals, Inc. US5705499, 1998, A
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