ChemicalBook CAS DataBase List 4-Bromo-2-nitrophenol

4-Bromo-2-nitrophenol synthesis

13synthesis methods

Product Name:4-Bromo-2-nitrophenol
CAS Number:7693-52-9
Molecular formula:C6H4BrNO3
Molecular Weight:218

88-75-5
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$15.00/5mg

7693-52-9
230 suppliers
$5.00/1g

Yield:7693-52-9 100%

Reaction Conditions:

with sulfuric acid;C₂₀H₂₂Br₂N₂O₅V;dihydrogen peroxide in methanol;lithium hydroxide monohydrate at 20; for 0.583333 h;Catalytic behavior;Reagent/catalyst;Solvent;

Steps:

2.5. General procedure of the oxidative bromination reaction

General procedure: In a 10-mL round-bottom flask equipped with a magnetic stirring bar, 1 mM of the 2-nitrophenol was reacted with different amounts of the oxidant, acid, bromide source, and the vanadyl Schiff base complex in 4 mL of solvent. The content was stirred at room temperature.The progress of the reaction was monitored by GLC.

References:

Grivani, Gholamhossein;Tahmasebi, Vida;Khalaji, Aliakbar Dehno;Eigner, Václav;Du?ek, Michal [Journal of Coordination Chemistry,2014,vol. 67,# 22,p. 3664 - 3677]

80-35-3 Synthesis