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ChemicalBook CAS DataBase List 4-CHLORO-2-METHYL-3-NITROBENZOTRIFLUORIDE

4-CHLORO-2-METHYL-3-NITROBENZOTRIFLUORIDE synthesis

4synthesis methods
476660-41-0 Synthesis
4-Chloro-2-methyl-5-nitrobenzoic acid 97+%

476660-41-0
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Yield:18018-35-4 63%

Reaction Conditions:

with sulfur tetrafluoride;hydrogen fluoride at 85; for 24 h;Autoclave;Inert atmosphere;

References:

Alekseenko, Anatoliy N.;Bugera, Maksym Ya.;Gerus, Igor I.;Kiriakov, Oleksandr;Klipkov, Anton A.;Mykhailiuk, Pavel K.;Pustovit, Yurii;Razhyk, Bohdan;Semenov, Sergey;Starova, Viktoriia S.;Tananaiko, Oksana Yu.;Tarasenko, Karen;Tolmachev, Andrei A.;Trofymchuk, Serhii;Zaporozhets, Olga A. [Journal of Organic Chemistry,2020,vol. 85,# 5,p. 3110 - 3124]

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