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ChemicalBook CAS DataBase List (4-Chlorosulfonylphenoxy)acetic acid methyl ester

(4-Chlorosulfonylphenoxy)acetic acid methyl ester synthesis

3synthesis methods
-

Yield:56077-78-2 83%

Reaction Conditions:

Stage #1: methyl 2-phenoxyacetatewith chlorosulfonic acid at -5 - 20;Inert atmosphere;
Stage #2: methanol in dichloromethane at 0 - 20; for 1.25 h;Inert atmosphere;

References:

Shin, Jai Moo;Sachs, George;Cho, Young-Moon;Garst, Michael [Molecules,2009,vol. 14,# 12,p. 5247 - 5280] Location in patent:experimental part

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