![](/CAS/GIF/101-41-7.gif)
Methyl phenylacetate synthesis
- Product Name:Methyl phenylacetate
- CAS Number:101-41-7
- Molecular formula:C9H10O2
- Molecular Weight:150.17
![Dimethyl carbonate](/CAS/GIF/616-38-6.gif)
616-38-6
662 suppliers
$5.00/5G
![Phenylacetone](/CAS/GIF/103-79-7.gif)
103-79-7
1 suppliers
$28.00/10mg
![Methyl phenylacetate](/CAS/GIF/101-41-7.gif)
101-41-7
495 suppliers
$16.80/100ML
Yield:101-41-7 100%
Reaction Conditions:
with Novozym 435;acylase I from Aspergillus melleus;amano lipase AK from pseudomonas fluorescens;lipase from wheat germ;papaine in toluene at 40; for 48 h;Mechanism;Enzymatic reaction;
Steps:
4.3. Experimental setup
General procedure: To the solution of acid (1 mmol) in toluene (1 ml), the corresponding dialkyl carbonate (2 mmol) and enzymes (per 4 mg of each enzyme) were added in 5 ml vial. The reaction mixture was stirring for 24 or 48 h at 40 °C in vortex mixture (Heidolph Promax 1020) equipped with incubator (Heidolph Inkubator 1000). After cooling, the mixture was washed with NaHCO3 (3×) and brine (1×). Organic solvent was removed under vacuum to obtain the product 2a-2r.
References:
Zysk, Malgorzata;Zadlo, Anna;Brodzka, Anna;Wisniewska, Catalina;Ostaszewski, Ryszard [Journal of Molecular Catalysis B: Enzymatic,2014,vol. 102,p. 225 - 229]
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
737 suppliers
$9.00/25ml
![Phenethyl alcohol](/CAS/GIF/60-12-8.gif)
60-12-8
553 suppliers
$6.00/25g
![Methyl phenylacetate](/CAS/GIF/101-41-7.gif)
101-41-7
495 suppliers
$16.80/100ML
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
737 suppliers
$9.00/25ml
201230-82-2
1 suppliers
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![Benzyl bromide](/CAS/GIF/100-39-0.gif)
100-39-0
423 suppliers
$10.00/10g
![Methyl phenylacetate](/CAS/GIF/101-41-7.gif)
101-41-7
495 suppliers
$16.80/100ML
![Benzeneacetic acid, 4-[(methylsulfonyl)oxy]-, methyl ester](/CAS/20200515/GIF/539814-10-3.gif)
539814-10-3
0 suppliers
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![Methyl phenylacetate](/CAS/GIF/101-41-7.gif)
101-41-7
495 suppliers
$16.80/100ML
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
737 suppliers
$9.00/25ml
201230-82-2
1 suppliers
inquiry
![Toluene](/CAS/GIF/108-88-3.gif)
108-88-3
7 suppliers
$14.00/100ml
![Methyl phenylacetate](/CAS/GIF/101-41-7.gif)
101-41-7
495 suppliers
$16.80/100ML