4-(cyclohexyloxy)aniline synthesis
- Product Name:4-(cyclohexyloxy)aniline
- CAS Number:39905-48-1
- Molecular formula:C12H17NO
- Molecular Weight:191.27
108-85-0
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5493-73-2
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$698.00/5g
39905-48-1
53 suppliers
$45.00/25mg
Yield:39905-48-1 700 mg
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in methanol; for 16 h;
Steps:
71.b (b) 4-(Cyclohexyloxy)aniline
A stirred solution of 1 -(cyclohexyloxy)-4-nitrobenzene (1 g) in MeOH (15 mL) was purged with nitrogen and 10% Pd/C (0.721 g) was added. The reaction mixture was stirred for 16 ht under a hydrogen atmosphere (balloon). The reaction mixture was filtered through Celite and the filtrate was concentrated under reduced pressure to afford the titled compound (700 mg). LCMS m/z 192.1 (M+H)+.
References:
WO2017/153952,2017,A1 Location in patent:Page/Page column 147
5493-73-2
7 suppliers
$698.00/5g
39905-48-1
53 suppliers
$45.00/25mg
108-85-0
340 suppliers
$5.00/10g
39905-48-1
53 suppliers
$45.00/25mg
824-78-2
5 suppliers
$14.00/1g
39905-48-1
53 suppliers
$45.00/25mg
108-85-0
340 suppliers
$5.00/10g
123-30-8
617 suppliers
$10.00/5g
39905-48-1
53 suppliers
$45.00/25mg