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4-ETHYLSULFONYLACETOPHENONE synthesis

3synthesis methods
13329-40-3 Synthesis
4'-Iodoacetophenone

13329-40-3
266 suppliers
$6.00/5g

20035-08-9 Synthesis
Sodium ethanesulfinate

20035-08-9
122 suppliers
$10.00/1g

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Yield:99186-50-2 40%

Reaction Conditions:

with tetrakis(actonitrile)copper(I) hexafluorophosphate;2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl in dimethyl sulfoxide; for 16 h;Inert atmosphere;Irradiation;Schlenk technique;Heating;

References:

Cui, Wenwen;Jiang, Min;Lv, Jian;Song, Xiuyan;Sun, Kai;Xu, Guiyun;Yan, Qiuli;Yang, Daoshan [Organic Letters,2021,vol. 23,# 9,p. 3663 - 3668] Location in patent:supporting information

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