4-(ETHYLTHIO)ANILINE synthesis
- Product Name:4-(ETHYLTHIO)ANILINE
- CAS Number:3463-02-3
- Molecular formula:C8H11NS
- Molecular Weight:153.24
Yield:3463-02-3 92%
Reaction Conditions:
Stage #1: ethanethiolwith sodium hydride in tetrahydrofuran at 20; for 1 h;Inert atmosphere;
Stage #2: p-aminoiodobenzenewith di-μ-iodobis(tri-t-butylphosphino)dipalladium(l) in tetrahydrofuran;toluene at 40; for 3 h;Inert atmosphere;
References:
Scattolin, Thomas;Senol, Erdem;Yin, Guoyin;Guo, Qianqian;Schoenebeck, Franziska [Angewandte Chemie - International Edition,2018,vol. 57,# 38,p. 12425 - 12429][Angew. Chem.,2018,vol. 130,# 38,p. 12605 - 12609,5] Location in patent:supporting information
7205-60-9
16 suppliers
inquiry
3463-02-3
2 suppliers
inquiry
