4-fluoro-N-phenyl-benzenecarbothioamide synthesis
- Product Name:4-fluoro-N-phenyl-benzenecarbothioamide
- CAS Number:1629-19-2
- Molecular formula:C13H10FNS
- Molecular Weight:231.29
366-63-2
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Yield:-
Reaction Conditions:
with Lawessons reagent in toluene at 135; for 2 h;Inert atmosphere;Green chemistry;
Steps:
6.2
(2) Sampling was carried out according to the molar ratio of compound C to Lawson's reagent of 1:0.6, put into a 100 mL volumetric flask, added 20 mL of toluene, heated to 135 °C in an oil bath under nitrogen protection, and reacted for 2 h, Compound D is obtained by separating and purifying with the volume ratio of petroleum ether:ethyl acetate=4:1.
References:
CN113929658,2022,A Location in patent:Paragraph 0075-0079; 0081
62-53-3
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403-43-0
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