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ChemicalBook CAS DataBase List 4-METHOXYBENZOIC ACID-ALPHA-13C

4-METHOXYBENZOIC ACID-ALPHA-13C synthesis

4synthesis methods
-

Yield:69838-89-7 82%

Reaction Conditions:

Stage #1: para-iodoanisolewith tert.-butyl lithium in diethyl ether;pentane at -78; for 1.5 h;
Stage #2: carbon dioxide in diethyl ether;pentane at -40 - 20;Further stages.;

References:

Gable, Kevin P.;Zhuravlev, Fedor A. [Journal of the American Chemical Society,2002,vol. 124,# 15,p. 3970 - 3979]

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