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4-n-butylpropiophenone synthesis

5synthesis methods
85068-34-4 Synthesis
3',5'-BIS(TRIFLUOROMETHYL)PROPIOPHENONE

85068-34-4
94 suppliers
$8.00/1g

625458-85-7 Synthesis
4-Butylphenylboronic acid pinacol ester

625458-85-7
37 suppliers
$45.00/100mg

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Yield:79219-21-9 87 %

Reaction Conditions:

with [Rh(OH)(cod)]2;1,3-bis(2,6-dibenzhydryl-4-methylphenyl)-1H-imidazol-3-ium chloride;potassium tert-butylate;water;cesium fluoride in toluene at 150;Sealed tube;

References:

Huang, Jiangkun;Yan, Xufei;Xia, Ying [Angewandte Chemie - International Edition,2022,vol. 61,# 49,art. no. E202211080][Angew. Chem.,2022,vol. 134,# 49] Location in patent:supporting information