(4-PHENYLAMINOCARBONYLPHENYL)BORONIC ACID synthesis
- Product Name:(4-PHENYLAMINOCARBONYLPHENYL)BORONIC ACID
- CAS Number:330793-45-8
- Molecular formula:C13H12BNO3
- Molecular Weight:241.05
14047-29-1
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330793-45-8
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Yield: 67%
Reaction Conditions:
Stage #1:4-carboxyphenylboronic acid with N,N-diethanolaminomethyl polystyrene in tetrahydrofuran at 20; for 1 h;
Stage #2:aniline with water;benzotriazol-1-ol;diisopropyl-carbodiimide at 20; for 18 h;
Stage #3: in tetrahydrofuran;water at 20; for 0.0166667 h;Further stages.;
References:
Gravel, Michael;Thompson, Kim A.;Zak, Mark;Berube, Christian;Hall, Dennis G. [Journal of Organic Chemistry,2002,vol. 67,# 1,p. 3 - 15]