4-TERT-BUTYL-PHENYL-HYDRAZINE synthesis
- Product Name:4-TERT-BUTYL-PHENYL-HYDRAZINE
- CAS Number:61765-93-3
- Molecular formula:C10H16N2
- Molecular Weight:164.25
3972-65-4
320 suppliers
$8.00/10g
61765-93-3
18 suppliers
inquiry
Yield:-
Reaction Conditions:
Stage #1:1-bromo-4-tert-butylbenzene with t-butoxycarbonylhydrazine;t-BuBrettPhos;[tBuBrettPhosPd(allyl)]OTf;sodium t-butanolate in water at 45; for 1.5 h;Inert atmosphere;
Stage #2: with sulfuric acid in ethanol;water at 90 - 95;Inert atmosphere;Sealed tube;
References:
Akporji, Nnamdi;Braga, Felipe C.;Gabriel, Christopher M.;Landstrom, Evan B.;Lee, Nicholas R.;Lipshutz, Bruce H. [Organic Letters,2020] Location in patent:supporting information
3972-56-3
129 suppliers
$14.00/1g
61765-93-3
18 suppliers
inquiry
7598-28-9
3 suppliers
$57.00/50mg
61765-93-3
18 suppliers
inquiry
769-92-6
284 suppliers
$6.00/10g
61765-93-3
18 suppliers
inquiry