1,2-Ethanedione, 1-[2,3-dihydro-1-(MethoxyiMino)-1H-inden-5-yl]-2-(4-pyridinyl)- synthesis

5synthesis methods

Product Name:1,2-Ethanedione, 1-[2,3-dihydro-1-(MethoxyiMino)-1H-inden-5-yl]-2-(4-pyridinyl)-
CAS Number:405554-66-7
Molecular formula:C17H14N2O3
Molecular Weight:294.3

1H-Indene-5-carboxaldehyde, 2,3-dihydro-1-(MethoxyiMino)-

405554-63-4
4 suppliers
inquiry

1,2-Ethanedione, 1-[2,3-dihydro-1-(MethoxyiMino)-1H-inden-5-yl]-2-(4-pyridinyl)-

405554-66-7
8 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: LDA / tetrahydrofuran / -60 °C
1.2: tetrahydrofuran / -60 °C
2.1: TBAF / tetrahydrofuran
3.1: 94 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / -60 - 20 °C

References:

Takle, Andrew K.;Brown, Murray J.B.;Davies, Susannah;Dean, David K.;Francis, Gerraint;Gaiba, Alessandra;Hird, Alex W.;King, Frank D.;Lovell, Peter J.;Naylor, Antoinette;Reith, Alastair D.;Steadman, Jon G.;Wilson, David M. [Bioorganic and Medicinal Chemistry Letters,2006,vol. 16,# 2,p. 378 - 381]

405554-64-5 Synthesis

1H-Inden-1-one, 5-[1,2-dihydroxy-2-(4-pyridinyl)ethyl]-2,3-dihydro-, O-MethyloxiMe

405554-64-5
7 suppliers
inquiry

405554-66-7
8 suppliers
inquiry

References

1H-Inden-1-one, 5-broMo-2,3-dihydro-, O-MethyloxiMe

405554-62-3
8 suppliers
inquiry

405554-66-7
8 suppliers
inquiry

References

1H-Inden-1-one, 5-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-hydroxy-2-(4-pyridinyl)ethyl]-2,3-dihydro-, O-methyloxime

405554-65-6
0 suppliers
inquiry

405554-66-7
8 suppliers
inquiry

References

34598-49-7 Synthesis

34598-49-7
368 suppliers
$14.00/5g

405554-66-7
8 suppliers
inquiry

References