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ChemicalBook CAS DataBase List 4'-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl-4-carbonitrile

4'-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl-4-carbonitrile synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; methanol; toluene / 22 h / 80 °C / Inert atmosphere
2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / N,N-dimethyl-formamide / 2.5 h / 80 °C / Inert atmosphere

References:

Oesch, David;Luedtke, Nathan W. [Chemical Communications,2015,vol. 51,# 63,p. 12641 - 12644]

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