4'-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl-4-carbonitrile synthesis
- Product Name:4'-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)biphenyl-4-carbonitrile
- CAS Number:406482-72-2
- Molecular formula:C19H20BNO2
- Molecular Weight:305.18
5467-74-3
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; methanol; toluene / 22 h / 80 °C / Inert atmosphere
2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / N,N-dimethyl-formamide / 2.5 h / 80 °C / Inert atmosphere
References:
Oesch, David;Luedtke, Nathan W. [Chemical Communications,2015,vol. 51,# 63,p. 12641 - 12644]
50670-50-3
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73183-34-3
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106-37-6
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3058-39-7
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