ChemicalBook CAS DataBase List 8-methoxy-2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole

8-methoxy-2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole synthesis

12synthesis methods

Product Name:8-methoxy-2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole
CAS Number:41505-84-4
Molecular formula:C13H16N2O
Molecular Weight:216.28

923293-14-5 Synthesis

923293-14-5
7 suppliers
inquiry

8-methoxy-2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole

41505-84-4
9 suppliers
$45.00/50mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: acetic acid; sodium nitrite / water / 1.5 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: dichloromethane / 20 °C / Inert atmosphere
3.1: ruthenium trichloride hydrate / Isopropyl acetate / 15 h / 80 °C / Inert atmosphere
4.1: sodium tetrahydroborate / methanol; water / 20 - 100 °C / Inert atmosphere

References:

Dong, Huijun;Latka, Regina T.;Driver, Tom G. [Organic Letters,2011,vol. 13,# 10,p. 2726 - 2729]