ChemicalBook CAS DataBase List 1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose

1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose synthesis

3synthesis methods

Product Name:1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose
CAS Number:443642-30-6
Molecular formula:C20H18Cl4O5
Molecular Weight:480.17

1-Methyl-3,5-bis-O-(2,4-dichlorobenzyl)-alpha-D-ribofuranoside

168427-35-8
53 suppliers
$45.00/250mg

1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose

443642-30-6
49 suppliers
$75.00/50mg

Yield:443642-30-6 90%

Reaction Conditions:

Stage #1: (3R,4S,5R)-4-((2,4-dichlorobenzyl)oxy)-5-(((2,4-dichlorobenzyl)oxy)methyl)-2-methoxytetrahydrofuran-3-olwith trichloroisocyanuric acid in dichloromethane at 0; for 0.166667 h;Inert atmosphere;
Stage #2: with 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical in dichloromethane at 20; for 3 h;Inert atmosphere;

References:

Zeng, Debin;Zhang, Rui;Nie, Quandeng;Cao, Lin;Shang, Luqing;Yin, Zheng [ACS Medicinal Chemistry Letters,2016,vol. 7,# 12,p. 1197 - 1201] Location in patent:supporting information

Methyl 2,3,5-tris-O-(2,4-dichlorobenzyl)-D-ribofuranoside

677299-16-0
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443642-30-6
49 suppliers
$75.00/50mg

References

Methyl 2'-O-acetyl-3,5-bis-O-(2,4-dichlorobenzyl)-alpha-D-ribofuranoside

168427-36-9
0 suppliers
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443642-30-6
49 suppliers
$75.00/50mg

References

1-O-Methyl-3,5-bis-O-[(2,4-dichlorophenyl)methyl]-alpha-D-erthro-pentofuranoside-2-ulose Related Search:

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