5-[1-(2,3-DiMethylphenyl)ethenyl]iMidazole synthesis
- Product Name:5-[1-(2,3-DiMethylphenyl)ethenyl]iMidazole
- CAS Number:1021949-47-2
- Molecular formula:C13H14N2
- Molecular Weight:198.26
5779-93-1
257 suppliers
$12.00/1g
1021949-47-2
106 suppliers
$65.00/100mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: magnesium; iodine / tetrahydrofuran / 35 - 65 °C / Inert atmosphere
1.2: 6 h / 20 - 25 °C
2.1: Dess-Martin periodane; magnesium sulfate / dichloromethane / 12 h / 20 - 30 °C
3.1: potassium tert-butylate / tetrahydrofuran / 18 h / 20 - 25 °C
References:
Jiangsu Zhengda Qingjiang Pharmaceutical Co., Ltd.;Meng Fanke;Chong Qinglei;Li Mingfeng;Li Xianzhe;Li Zhiming CN107857731, 2018, A
176721-03-2
52 suppliers
$105.00/10mg
1021949-47-2
106 suppliers
$65.00/100mg
576-23-8
263 suppliers
$16.00/25 g
1021949-47-2
106 suppliers
$65.00/100mg
176721-01-0
59 suppliers
$62.00/100mg
1021949-47-2
106 suppliers
$65.00/100mg
![(2,3-Dimethylphenyl)[1-(trityl)-1H-imidazol-4-yl]methanone](/CAS2/GIF/176721-02-1.gif)
176721-02-1
72 suppliers
$110.09/10 mg
1021949-47-2
106 suppliers
$65.00/100mg