ChemicalBook CAS DataBase List [5-(2-FURYL)-1-METHYL-1H-PYRAZOL-3-YL]METHANOL

[5-(2-FURYL)-1-METHYL-1H-PYRAZOL-3-YL]METHANOL synthesis

3synthesis methods

Product Name:[5-(2-FURYL)-1-METHYL-1H-PYRAZOL-3-YL]METHANOL
CAS Number:876728-41-5
Molecular formula:C9H10N2O2
Molecular Weight:178.19

ETHYL 5-(2-FURYL)-1-METHYL-1H-PYRAZOLE-3-CARBOXYLATE

104296-35-7
25 suppliers
$110.00/100mg

[5-(2-FURYL)-1-METHYL-1H-PYRAZOL-3-YL]METHANOL

876728-41-5
20 suppliers
$85.00/250mg

Yield:876728-41-5 98%

Reaction Conditions:

Stage #1: ethyl 5-(furan-2-yl)-1-methyl-1H-pyrazole-3-carboxylatewith lithium aluminium tetrahydride in tetrahydrofuran at 0 - 60; for 1 h;Inert atmosphere;
Stage #2: with sodium hydroxide;water at 0 - 20;

References:

Fustero, Santos;Roman, Raquel;Sanz-Cervera, Juan F.;Simon-Fuentes, Antonio;Bueno, Jorge;Villanova, Salvador [Journal of Organic Chemistry,2008,vol. 73,# 21,p. 8545 - 8552] Location in patent:experimental part

1192-62-7
491 suppliers
$5.00/10g

876728-41-5
20 suppliers
$85.00/250mg

References

2-Furanbutanoic acid, α,γ-dioxo-, ethyl ester

36983-35-4
12 suppliers
$45.00/10mg

876728-41-5
20 suppliers
$85.00/250mg

References

[5-(2-FURYL)-1-METHYL-1H-PYRAZOL-3-YL]METHANOL Related Search:

5-(2-FURYL)-1-PHENYL-1H-PYRAZOLE-3-CARBOXYLIC ACID