5,6-DIMETHOXY-1,3-BENZODIOXOLE synthesis
- Product Name:5,6-DIMETHOXY-1,3-BENZODIOXOLE
- CAS Number:3214-12-8
- Molecular formula:C9H10O4
- Molecular Weight:182.17
533-31-3
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3214-12-8
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$100.00/100mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: anh. K2CO3 / acetone / Heating
2: phosphorus oxychloride / chlorobenzene / 24 h / Ambient temperature
3: 80 percent / 85percent formic acid; 30percent H2O2 / 16 h / 5 °C
4: anh. K2CO3 / acetone / 6 h / Heating
References:
Devakumar, C.;Saxena, V. S.;Mukerjee, S. K. [Agricultural and Biological Chemistry,1985,vol. 49,# 3,p. 725 - 730]