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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

5-BroMo-4-hydrazinylthieno[2,3-d]pyriMidine synthesis

4synthesis methods
4651-82-5 Synthesis
2-AMINO-3-CYANOTHIOPHENE

4651-82-5
182 suppliers
$7.00/1g

5-BroMo-4-hydrazinylthieno[2,3-d]pyriMidine

1239460-84-4
1 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 5 steps
1: sulfuric acid / 0.25 h / 100 °C / Microwave irradiation
2: bromine; sodium acetate / acetic acid / Reflux
3: acetic acid; zinc / water
4: trichlorophosphate / 0.5 h / 100 °C / Microwave irradiation
5: hydrazine / ethanol / 75 °C

References:

Bowers, Simeon;Truong, Anh P.;Jeffrey Neitz;Hom, Roy K.;Sealy, Jennifer M.;Probst, Gary D.;Quincy, David;Peterson, Brian;Chan, Wayman;Galemmo Jr., Robert A.;Konradi, Andrei W.;Sham, Hing L.;Tóth, Gergely;Pan, Hu;Lin, May;Yao, Nanhua;Artis, Dean R.;Zhang, Heather;Chen, Linda;Dryer, Mark;Samant, Bhushan;Zmolek, Wes;Wong, Karina;Lorentzen, Colin;Goldbach, Erich;Tonn, George;Quinn, Kevin P.;Sauer, John-Michael;Wright, Sarah;Powell, Kyle;Ruslim, Lany;Ren, Zhao;Bard, Frédérique;Yednock, Ted A.;Griswold-Prenner, Irene [Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,# 18,p. 5521 - 5527]

814918-95-1 Synthesis
5-bromo-4-chlorothieno[2,3-d]pyrimidine

814918-95-1
97 suppliers
$77.00/100mg

5-BroMo-4-hydrazinylthieno[2,3-d]pyriMidine

1239460-84-4
1 suppliers
inquiry

References
1239460-82-2 Synthesis
5,6-DibroMothieno[2,3-d]pyriMidin-4(3H)-one

1239460-82-2
18 suppliers
inquiry

5-BroMo-4-hydrazinylthieno[2,3-d]pyriMidine

1239460-84-4
1 suppliers
inquiry

References
Thieno[2,3-d]pyrimidin-4(3H)one

14080-50-3
180 suppliers
$9.00/250mg

5-BroMo-4-hydrazinylthieno[2,3-d]pyriMidine

1239460-84-4
1 suppliers
inquiry

References