5-bromo-4-methylnicotinonitrile synthesis
- Product Name:5-bromo-4-methylnicotinonitrile
- CAS Number:890092-52-1
- Molecular formula:C7H5BrN2
- Molecular Weight:197.03
3430-23-7
192 suppliers
$5.00/250mg
105-56-6
431 suppliers
$10.00/5ml
890092-52-1
52 suppliers
inquiry
Yield: 48%
Reaction Conditions:
with N,N,N,N,-tetramethylethylenediamine;palladium diacetate;sodium hydride;1,2-bis-(diphenylphosphino)ethane;potassium iodide in N,N-dimethyl-formamide at 130; for 22 h;Inert atmosphere;
References:
Zheng, Shuyan;Yu, Chunhui;Shen, Zhengwu [Organic Letters,2012,vol. 14,# 14,p. 3644 - 3647] Location in patent:supporting information; experimental part