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ChemicalBook CAS DataBase List 5-Fluoro-2-iodo-1,3-dimethylbenzene

5-Fluoro-2-iodo-1,3-dimethylbenzene synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: (i) PCl5, (ii) aq. NH3
2: aq. NaOH, Br2
3: (i) aq. HCl, NaNO2, (ii) HPF6
4: H2 / Pd-C
5: (i) H2SO4, NaNO2, (ii) KI

References:

Dewar,M.J.S.;Takeuchi,Y. [Journal of the American Chemical Society,1967,vol. 89,# 2,p. 390 - 394]