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5-METHYL-[5'-13C]URIDINE synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: H2SO4; AcOH / 3 h / 0 °C
2: 98 percent / trimethylsilyl trifluoromethanesulfonate / CHCl3
3: NaOH; pyridine / methanol; H2O

References:

Kawashima, Etsuko;Umabe, Kaoru;Sekine, Takeshi [Journal of Organic Chemistry,2002,vol. 67,# 15,p. 5142 - 5151]

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