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ChemicalBook CAS DataBase List 5-METHYL-[1',2',3',4',5'-13C5]URIDINE

5-METHYL-[1',2',3',4',5'-13C5]URIDINE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 7 steps
1: 94 percent / PDC, Ac2O / CH2Cl2 / Heating
2: H5IO6 / ethyl acetate
3: NaBH4 / ethanol
4: 95 percent / Py
5: 80 percent / tetrahydrofuran
6: TMSOTf / 1,2-dichloro-ethane / 0 °C
7: 48 percent / NH3 / methanol

References:

Agrofoglio, Luigi A.;Jacquinet, Jean-Claude;Lancelot, Gerard [Tetrahedron Letters,1997,vol. 38,# 8,p. 1411 - 1412]

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