![](/CAS/GIF/201996-60-3.gif)
5-METHYL-[1'-13C]URIDINE synthesis
- Product Name:5-METHYL-[1'-13C]URIDINE
- CAS Number:201996-60-3
- Molecular formula:C10H14N2O6
- Molecular Weight:259.24
![D-Ribofuranoside-1-13C, methyl, tribenzoate (9CI)](/CAS/20180703/GIF/380611-22-3.gif)
380611-22-3
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![5-METHYL-[1'-13C]URIDINE](/CAS/GIF/201996-60-3.gif)
201996-60-3
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$165.00/5mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 95 percent / BF3*Et2O / CH2Cl2 / 1 h / 0 °C
2: 95 percent / m-CPBA, NaHCO3 / CH2Cl2 / 1 h / 0 °C
3: 1) hexamethyldisilazane, 2) TMSOTf / 1) 2 h, reflux, 2) 1,2-dichloroethane, 5 min, r.t.
4: 2M NaOH, pyridine / methanol / 0.08 h / 0 °C
References:
Chanteloup, Luc;Beau, Jean-Marie [Tetrahedron Letters,1992,vol. 33,# 37,p. 5347 - 5350]