ChemicalBook CAS DataBase List 5-METHYL-[1'-13C]URIDINE

5-METHYL-[1'-13C]URIDINE synthesis

1synthesis methods

Product Name:5-METHYL-[1'-13C]URIDINE
CAS Number:201996-60-3
Molecular formula:C10H14N2O6
Molecular Weight:259.24

D-Ribofuranoside-1-13C, methyl, tribenzoate (9CI)

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 95 percent / BF₃*Et₂O / CH₂Cl₂ / 1 h / 0 °C
2: 95 percent / m-CPBA, NaHCO₃ / CH₂Cl₂ / 1 h / 0 °C
3: 1) hexamethyldisilazane, 2) TMSOTf / 1) 2 h, reflux, 2) 1,2-dichloroethane, 5 min, r.t.
4: 2M NaOH, pyridine / methanol / 0.08 h / 0 °C

References:

Chanteloup, Luc;Beau, Jean-Marie [Tetrahedron Letters,1992,vol. 33,# 37,p. 5347 - 5350]

5-METHYL-[1'-13C]URIDINE Related Search:

URIDINE (RIBOSE-1-13C) 5-METHYL-[1',2',3',4',5'-13C5]URIDINE 5-Methyluridine Ribose